Photon energy | 1486.61eV |
Spectrum type | survey |
Resolution | 150 |
Lens Mode | SmallArea |
Dwell Time | 0.1 |
Step size | 0.4 |
Number of scans | 1 |
Name | 4. CuO, in 0.1 mbar O2, 300 C |
Ex situ preparation | Mechanical polishing down to 0.05 microns. Mounted with thermocouple onto a stainless steel sample holder. |
In situ preparation | Sputter cleaned with Ar ion beam to remove C and O. Annealed in vacuum to 700 C. Heated to 200 C in 0.1 mbar O2 for 8 hours. Increased temperature to 300 C. |
Additional Information | These spectra were measured after the sample had been transformed to CuO. The data set represents an average of spectra measured over 1.5 hours. |
Measurement Date | 02-02-2174 |
Condition | Value | Units |
---|---|---|
pressure | 0.1 | mbar |
temperature | 300 | C |
ambient composition | O2 | none |
Analyzer Mode | FAT |
Area | 0.3 mm diameter |
Strength | 70 W |
Source Beam Size | 0.3 mm diameter |
Take Off Angle | 90 degrees |
Analyzer Acceptance Angle | 22 degrees |
Laboratory | Surface Analytics |
Instrument | Phoibos NAP-150 |
Protocol | ISO 15472:2010 |
Calibration date | 04-01-2018 |
Binding Energy | 83.98 |
Emission line | Au 4f7/2 |