| Photon energy | 1486.61eV |
| Spectrum type | Pd 3d |
| Resolution | 20 |
| Lens Mode | ARM22 |
| Dwell Time | 0.1 |
| Step size | 0.1 |
| Number of scans | 1 |
| Name | Pd in 1 mbar O2 520°C |
| Ex situ preparation | piece of a 0.1 mm thick polycristalline Pd foil (Alfa Aesar, 99,9% purity) |
| In situ preparation | cleaned by several Ar+ sputtering and annealing cycles (in 0.5 mbar O2). After Ar+ sputter cleaning the sample was reduced in 0.5 mbar H2 at 450°C for 2h. |
| Additional Information | The sample was heated in 1 mbar O2 (70°C-750°C) with a heating rate of 0.4°C/min |
| Measurement Date | 02-10-2020 |
| Condition | Value | Units |
|---|---|---|
| O2 pressure | 1 | mbar |
| Temperature | 520 | °C |
| Analyzer Mode | FAT |
| Area | 0,8 |
| Strength | 180W |
| Source Beam Size | 0,8 |
| Take Off Angle | 90 |
| Analyzer Acceptance Angle | 22 |
| Laboratory | Surface Analytics |
| Instrument | Phoibos NAP-150 |
| Protocol | ISO 15472:2010 |
| Calibration date | 30-09-2020 |
| Binding Energy | 368.18 |
| Emission line | Ag 3d5/2 |
