| Photon energy | 1486.61eV |
| Spectrum type | survey |
| Resolution | 69.902 |
| Lens Mode | ARM22 |
| Dwell Time | 0.1 |
| Step size | 1 |
| Number of scans | 2 |
| Name | Ag0.95Pd0.05 |
| Ex situ preparation | Quantitative amounts of the Ag (slugs 3×3mm, 99.99%) and Pd (granules <7mm, 99.95%) purchased from EvoChem were melted in a light oven, with a four times re-melting process for homogenization. Afterwards the alloy was cold-rolled to a 1.6 mm thick foil and then annealed for 6h at 800°C for grain size growth. The foil was cut into smaller pieces and polished, with incrementally finer grid, down to a 1 µm using diamond suspension. |
| In situ preparation | Ar+ sputter and annealing cycles for cleaning. The reference spectra are measured directly after sputtering in UHV |
| Measurement Date | 07-06-2020 |
| Condition | Value | Units |
|---|---|---|
| pressure | 1E-8 | mbar |
| Analyzer Mode | FAT |
| Area | 0,8 |
| Strength | 150W |
| Source Beam Size | 0,8 |
| Take Off Angle | 90 |
| Analyzer Acceptance Angle | 22 |
| Laboratory | Surface Analytics |
| Instrument | Phoibos NAP-150 |
| Protocol | ISO 15472:2010 |
| Calibration date | 27-04-2020 |
| Binding Energy | 83.96 |
| Emission line | Au 4f7/2 |
| Binding Energy | 932.63 |
| Emission line | Cu 2p3/2 |
| Binding Energy | 368.22 |
| Emission line | Ag 3d5/2 |
