Measurement Data
General Info
Phoibos NAP-150
reference spectra of Ag0.98Pd0.02 and Ag0.95Pd0.05
https://doi.org/10.5281/zenodo.4482000
Contributors
Profile picture of Mark Greiner
Mark Greiner
Contributor
Profile picture of Caroline Hartwig
Caroline Hartwig
Owner
No
Element; Emission line;
Photon energy 1486.61eV
Spectrum type survey
Resolution 69.902
Lens Mode ARM22
Dwell Time 0.1
Step size 1
Number of scans 2
Sample Info
Ag0.95Pd0.05
Quantitative amounts of the Ag (slugs 3×3mm, 99.99%) and Pd (granules <7mm, 99.95%) purchased from EvoChem were melted in a light oven, with a four times re-melting process for homogenization. Afterwards the alloy was cold-rolled to a 1.6 mm thick foil and then annealed for 6h at 800°C for grain size growth. The foil was cut into smaller pieces and polished, with incrementally finer grid, down to a 1 µm using diamond suspension.
Ar+ sputter and annealing cycles for cleaning. The reference spectra are measured directly after sputtering in UHV
Pd
Ag
foil
Dataset Info

This will generate DOI for a single dataset
3
07-06-2020
Conditions
pressure
1E-8
mbar

Spectrometer Settings
FAT
0,8
150W
0,8
90
22
No
Element; Emission line;
Photon energy 1486.61eV
Spectrum type survey
Resolution 100
Lens Mode LA
Dwell Time 0.1
Step size 1
Number of scans 3
Sample Info
Ag0.98Pd0.02
Quantitative amounts of the Ag (slugs 3×3mm, 99.99%) and Pd (granules <7mm, 99.95%) purchased from EvoChem were melted in a light oven, with a four times re-melting process for homogenization. Afterwards the alloy was cold-rolled to a 1.6 mm thick foil and then annealed for 6h at 800°C for grain size growth. The foil was cut into smaller pieces and polished, with incrementally finer grid, down to a 1 µm using diamond suspension.
Ar+ sputter and annealing cycles for cleaning. The reference spectra are measured directly after sputtering in UHV
Ag
Pd
foil
Dataset Info

This will generate DOI for a single dataset
3
09-09-2020
Calibration
ISO 15472:2010
Au 4f7/2
83.96
Cu 2p3/2
932.63
Ag 3d5/2
368.22
27-04-2020
Conductive