Measurement Data
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General Info
Phoibos NAP-150
Au, Ag, Cu in He
https://doi.org/10.5281/zenodo.4020613
This data collection contains a comparison of spectra from Au, Ag and Cu foils measured with and without the presence of He in the atmosphere.
Contributors
Profile picture of Mark Greiner
Mark Greiner
Owner
No
Element; Emission line;
1
Ag MNN
2
Ag 3p
3
Ag 3d
4
Ag 4d
5
survey
Photon energy 1486.61eV
Spectrum type survey
Resolution 20
Dwell Time 0.9
Step size 0.5
Number of scans 1
Sample Info
1. Ag in vacuum
Clamped sample to stainless steel holder using stainless steel clips.
Sputter cleaned for 15 min using Ar at 3kV and a pressure of 1E-5 mbar
Measured from a Ag foil in vacuum, with the sample at a distance of 0.8 mm away from the nozzle. Nozzle diameter was 0.8 mm.
Ag
C
Ar
O
foil
Dataset Info

This will generate DOI for a single dataset
5
06-03-2020
Conditions
pressure
1E-8
mbar
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
Ag MNN
2
Ag 3p
3
Ag 3d
4
Ag 4d
5
survey
Photon energy 1486.61eV
Spectrum type survey
Resolution 20
Dwell Time 2.7
Step size 0.5
Number of scans 1
Sample Info
1. Ag in 4 mbar He
Clamped sample to stainless steel holder using stainless steel clips.
Sputter cleaned for 15 min using Ar at 3kV and a pressure of 1E-5 mbar
Measured from a Ag foil in 4 mbar of He, with the sample at a distance of 0.8 mm away from the nozzle. Nozzle diameter was 0.8 mm.
Ag
C
Ar
O
foil
Dataset Info

This will generate DOI for a single dataset
5
07-03-2020
Conditions
pressure
4
mbar
ambient composition
He
none
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
survey
2
Au 4f
3
Au 4d
4
Au 4p
Photon energy 1486.61eV
Spectrum type Au 4p
Resolution 20
Dwell Time 0.1
Step size 0.1
Number of scans 1
Sample Info
2. Au in 4 mbar He
Clamped sample to stainless steel holder using stainless steel clips.
Sputter cleaned for 15 min using Ar at 3kV and a pressure of 1E-5 mbar
Measured from a Au foil in 4 mbar of He, with the sample at a distance of 0.8 mm away from the nozzle. Nozzle diameter was 0.8 mm.
Au
C
Ar
foil
Dataset Info

This will generate DOI for a single dataset
4
10-03-2020
Conditions
pressure
4
mbar
ambient composition
He
none
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
survey
2
Au 4f
3
Au 4d
4
Au 4p
Photon energy 1486.61eV
Spectrum type Au 4p
Resolution 20
Dwell Time 0.1
Step size 0.1
Number of scans 1
Sample Info
2. Au in vacuum
Clamped sample to stainless steel holder using stainless steel clips.
Sputter cleaned for 15 min using Ar at 3kV and a pressure of 1E-5 mbar
Measured from a Au foil in vacuum, with the sample at a distance of 0.8 mm away from the nozzle. Nozzle diameter was 0.8 mm.
Au
C
Ar
foil
Dataset Info

This will generate DOI for a single dataset
4
10-03-2020
Conditions
pressure
1E-8
mbar
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
survey
2
Cu 2p
3
Cu LMM
4
Cu 3s
5
Cu 2s
Photon energy 1486.61eV
Spectrum type Cu 2s
Resolution 20
Dwell Time 0.2
Step size 0.1
Number of scans 1
Sample Info
3. Cu in 4mbar He
Clamped sample to stainless steel holder using stainless steel clips.
Sputter cleaned for 15 min using Ar at 3kV and a pressure of 1E-5 mbar
Measured from a Cu foil in 4 mbar of He, with the sample at a distance of 0.8 mm away from the nozzle. Nozzle diameter was 0.8 mm.
Cu
C
Ar
O
foil
Dataset Info

This will generate DOI for a single dataset
5
11-03-2020
Conditions
pressure
4
mbar
ambient composition
He
none
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
survey
2
Cu 2p
3
Cu LMM
4
Cu 3s
5
Cu 2s
Photon energy 1486.61eV
Spectrum type Cu 2s
Resolution 20
Dwell Time 0.2
Step size 0.1
Number of scans 1
Sample Info
3. Cu in vacuum
Clamped sample to stainless steel holder using stainless steel clips.
Sputter cleaned for 15 min using Ar at 3kV and a pressure of 1E-5 mbar
Measured from a Cu foil in vacuum, with the sample at a distance of 0.8 mm away from the nozzle. Nozzle diameter was 0.8 mm.
Cu
C
Ar
O
foil
Dataset Info

This will generate DOI for a single dataset
5
11-03-2020
Conditions
pressure
1E-8
mbar
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
Au 4f
Photon energy 1486.61eV
Spectrum type Au 4f
Resolution 20
Dwell Time 0.1
Step size 0.1
Number of scans 2
Sample Info
4. Au in 23 mbar He
Clamped sample to stainless steel holder using stainless steel clips.
Sputter cleaned for 15 min using Ar at 3kV and a pressure of 1E-5 mbar
Measured from a Au foil in 23 mbar of He, with the sample at a distance of 0.3 mm away from the nozzle. Nozzle diameter was 0.3 mm.
Au
C
Ar
foil
Dataset Info

This will generate DOI for a single dataset
1
30-08-2020
Conditions
pressure
23
mbar
ambient composition
He
none
temperature
25
C
Spectrometer Settings
FAT
0.3 mm diameter
100 W, 15 kV
0.3 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
Au 4f
Photon energy 1486.61eV
Spectrum type Au 4f
Resolution 20
Dwell Time 1
Step size 0.1
Number of scans 1
Sample Info
4. Au in vacuum
Clamped sample to stainless steel holder using stainless steel clips.
Measured from a Au foil in vacuum, with the sample at a distance of 0.3 mm away from the nozzle. Nozzle diameter was 0.3 mm.
Au
C
Ar
foil
Dataset Info

This will generate DOI for a single dataset
1
29-08-2020
Conditions
pressure
1E-8
mbar
temperature
25
C
Spectrometer Settings
FAT
0.3 mm diameter
100 W, 15 kV
0.3 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
Au 4f
Photon energy 1486.61eV
Spectrum type Au 4f
Resolution 20
Dwell Time 1
Step size 0.1
Number of scans 1
Sample Info
4. Au in 12 mbar He
Clamped sample to stainless steel holder using stainless steel clips.
Sputter cleaned for 15 min using Ar at 3kV and a pressure of 1E-5 mbar
Measured from a Au foil in 12 mbar of He, with the sample at a distance of 0.3 mm away from the nozzle. Nozzle diameter was 0.3 mm.
Au
C
Ar
foil
Dataset Info

This will generate DOI for a single dataset
1
30-08-2020
Conditions
pressure
12
mbar
ambient composition
He
none
temperature
25
C
Spectrometer Settings
FAT
0.3 mm diameter
100 W, 15 kV
0.3 mm diameter
90 degrees
22 degrees
Calibration
ISO 15472:2010
Au 4f7/2
83.96
Cu 2p3/2
932.62
17-08-2020
Conductive
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