Measurement Data
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General Info
Phoibos NAP-150
Au, Ag, Cu in N2
https://doi.org/10.5281/zenodo.4020615
This data collection contains spectra for examining the effect of inelastic scattering of photoelectrons by N2 gas in the sample atmosphere. Data sets in this data collection that have the same leading number belong together.
Contributors
Profile picture of Mark Greiner
Mark Greiner
Owner
No
Element; Emission line;
1
survey
2
Ag MNN
3
Ag 3p
4
Ag 3d
5
Ag 4d
Photon energy 1486.61eV
Spectrum type Ag 4d
Resolution 20
Dwell Time 2.9
Step size 0.1
Number of scans 1
Sample Info
1. Ag in 2 mbar N2
Sample clamped to stainless steel holder using stainless steel clamps
Sputter cleaned for 15 min using Ar at 3 kV and a pressure of 1E-5 mbar
Spectra from a Ag foil measured in 2 mbar N2. Distance of sample to nozzle was 0.8 mm. Nozzle diameter was 0.8 mm.
Ag
C
Ar
O
foil
Dataset Info

This will generate DOI for a single dataset
5
10-03-2020
Conditions
pressure
2
mbar
ambient composition
N2
none
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
Ag 3p
2
Ag 3d
3
Ag 4d
4
Ag MNN
5
survey
Photon energy 1486.61eV
Spectrum type survey
Resolution 20
Dwell Time 0.9
Step size 0.5
Number of scans 1
Sample Info
1. Ag in vacuum
Sample clamped to stainless steel holder using stainless steel clamps
Sputter cleaned for 15 min using Ar at 3 kV and a pressure of 1E-5 mbar
Spectra from a Ag foil measured in vacuum. Distance of sample to nozzle was 0.8 mm. Nozzle diameter was 0.8 mm.
Ag
C
Ar
O
foil
Dataset Info

This will generate DOI for a single dataset
5
06-03-2020
Conditions
pressure
1E-8
mbar
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
Cu 2p
2
Cu LMM
3
Cu 3s
4
survey
5
Cu 2s
6
Cu 2s
Photon energy 1486.61eV
Spectrum type Cu 2s
Resolution 20
Dwell Time 4
Step size 0.1
Number of scans 1
Sample Info
2. Cu in vacuum
Sample clamped to stainless steel holder using stainless steel clamps
Sputter cleaned for 15 min using Ar at 3 kV and a pressure of 1E-5 mbar
Spectra from a Cu foil measured in vacuum. Distance of sample to nozzle was 0.8 mm. Nozzle diameter was 0.8 mm.
Cu
C
Ar
O
foil
Dataset Info

This will generate DOI for a single dataset
6
08-03-2020
Conditions
pressure
1E-8
mbar
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
Cu 2p
2
Cu LMM
3
Cu 3s
4
survey
5
Cu 2s
6
Cu 2s
Photon energy 1486.61eV
Spectrum type Cu 2s
Resolution 20
Dwell Time 7.8
Step size 0.1
Number of scans 1
Sample Info
2. Cu in 2mbar N2
Sample clamped to stainless steel holder using stainless steel clamps
Sputter cleaned for 15 min using Ar at 3 kV and a pressure of 1E-5 mbar
Spectra from a Cu foil measured in 2 mbar N2. Distance of sample to nozzle was 0.8 mm. Nozzle diameter was 0.8 mm.
Cu
C
Ar
O
foil
Dataset Info

This will generate DOI for a single dataset
6
09-03-2020
Conditions
pressure
2
mbar
ambient composition
N2
none
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
survey
2
Au 4f
3
Au 4d
4
Au 4p
5
Au 4p
Photon energy 1486.61eV
Spectrum type Au 4p
Resolution 20
Dwell Time 3
Step size 0.1
Number of scans 1
Sample Info
3. Au in 2mbar N2
Sample clamped to stainless steel holder using stainless steel clamps
Sputter cleaned for 15 min using Ar at 3 kV and a pressure of 1E-5 mbar
Spectra from a Au foil measured in 2 mbar N2. Distance of sample to nozzle was 0.8 mm. Nozzle diameter was 0.8 mm.
Au
C
Ar
foil
Dataset Info

This will generate DOI for a single dataset
5
09-03-2020
Conditions
pressure
2
mbar
ambient composition
N2
none
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
survey
2
Au 4f
3
Au 4d
4
Au 4p
5
Au 4p
Photon energy 1486.61eV
Spectrum type Au 4p
Resolution 20
Dwell Time 2
Step size 0.1
Number of scans 1
Sample Info
3. Au in vacuum
Sample clamped to stainless steel holder using stainless steel clamps
Sputter cleaned for 15 min using Ar at 3 kV and a pressure of 1E-5 mbar
Spectra from a Au foil measured in vacuum. Distance of sample to nozzle was 0.8 mm. Nozzle diameter was 0.8 mm.
Au
C
Ar
foil
Dataset Info

This will generate DOI for a single dataset
5
08-03-2020
Conditions
pressure
1E-8
mbar
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameters
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
Calibration
ISO 15472:2010
Au 4f7/2
83.96
Cu 2p3/2
932.62
17-08-2020
Conductive
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