Measurement Data
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General Info
Phoibos NAP-150
SnO2 reduction in ethylene glycol
https://doi.org/10.5281/zenodo.4437711
This is data from an in-situ XPS experiment where the oxidized surface of Sn foil was reduced to metal by heating the foil to 150 C in 0.1 mbar of ethylene glycol.
Contributors
Profile picture of Mark Greiner
Mark Greiner
Owner
No
Element; Emission line;
1
Sn 3d
2
Sn 3d
3
O 1s
4
survey
5
C 1s
Photon energy 1486.61eV
Spectrum type C 1s
Resolution 20
Dwell Time 0.4
Step size 0.1
Number of scans 1
Sample Info
0. SnO2 as loaded
Sample as loaded from air.
SnO2
C
Sn
foil
thin film
Dataset Info

This will generate DOI for a single dataset
5
28-02-2020
Conditions
pressure
5E-9
mbar
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W
0.8 mm diameter
90
22
No
Element; Emission line;
1
Sn 3d
2
Sn 3d
Photon energy 1486.61eV
Spectrum type Sn 3d
Resolution 20
Dwell Time 0.1
Step size 0.05
Number of scans 5
Sample Info
1. SnO2 in 0.1 mbar ethyl-glycol at 150 C, t=0-7min.
Sn foil, with native oxide, at the beginning of heating in ethylene glycol.
SnO2
C
Sn
foil
thin film
Dataset Info

This will generate DOI for a single dataset
2
02-04-2196
Conditions
pressure
0.1
mbar
ambient composition
ethylene glycol
none
temperature
150
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W
0.8 mm diameter
90
22
No
Element; Emission line;
1
Sn 3d
2
Sn 3d
Photon energy 1486.61eV
Spectrum type Sn 3d
Resolution 20
Dwell Time 0.1
Step size 0.05
Number of scans 5
Sample Info
2. SnO2 in 0.1 mbar ethyl-glycol at 150 C, t=22min.
Sn foil with native oxide after 22 minutes of reduction in ethylene glycol.
SnO2
C
Sn
foil
thin film
Dataset Info

This will generate DOI for a single dataset
2
02-04-2196
Conditions
pressure
0.1
mbar
ambient composition
ethylene glycol
none
temperature
150
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W
0.8 mm diameter
90
22
No
Element; Emission line;
1
Sn 3d
2
Sn 3d
Photon energy 1486.61eV
Spectrum type Sn 3d
Resolution 20
Dwell Time 0.1
Step size 0.05
Number of scans 5
Sample Info
3. SnO2 in 0.1 mbar ethyl-glycol at 150 C, t=30min.
Sn foil with native oxide after 30 minutes of reduction in ethylene glycol.
SnO2
Sn
C
foil
thin film
Dataset Info

This will generate DOI for a single dataset
2
02-04-2196
Conditions
pressure
0.1
mbar
ambient composition
ethylene glycol
none
temperature
150
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W
0.8 mm diameter
90
22
No
Element; Emission line;
1
Sn 3d
2
Sn 3d
Photon energy 1486.61eV
Spectrum type Sn 3d
Resolution 20
Dwell Time 0.1
Step size 0.05
Number of scans 5
Sample Info
4. SnO2 in 0.1 mbar ethyl-glycol at 150 C, t=52.2min.
Sn foil with native oxide after 52 minutes of reduction in ethylene glycol.
SnO2
Sn
C
foil
thin film
Dataset Info

This will generate DOI for a single dataset
2
02-04-2196
Conditions
pressure
0.1
mbar
ambient composition
ethylene glycol
none
temperature
150
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
Sn 3d
2
Sn 3d
3
survey
4
O 1s
5
C 1s
Photon energy 1486.61eV
Spectrum type C 1s
Resolution 20
Dwell Time 0.8
Step size 0.1
Number of scans 1
Sample Info
5. SnO2 in 0.1 mbar ethyl-glycol at 150 C, t=114-130min.
Sn foil with native oxide after 114-130 minutes of reduction in ethylene glycol.
Sn
C
SnOx
foil
Dataset Info

This will generate DOI for a single dataset
5
02-04-2196
Conditions
pressure
0.1
mbar
ambient composition
ethylene glycol
none
temperature
150
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W
0.8 mm diameter
90 degrees
22 degrees
Calibration
ISO 15472:2010
Au 4f7/2
83.96
Cu 2p3/2
932.64
Ag 3d5/2
368.22
28-02-2020
Conductive
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