Measurement Data
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General Info
Phoibos NAP-150
Au, Ag, Cu in H2
https://doi.org/10.5281/zenodo.4020617
Spectra measured from Au, Ag and Cu with and without H2. The experiments investigate how inelastic scattering in the gas phase influences photoemission signal. Datasets that have the same leading number, belong together.
Contributors
Profile picture of Mark Greiner
Mark Greiner
Owner
No
Element; Emission line;
1
Ag MNN
2
Ag 3p
3
Ag 3d
4
Ag 4d
5
survey
Photon energy 1486.61eV
Spectrum type survey
Resolution 20
Dwell Time 1.9
Step size 0.5
Number of scans 1
Sample Info
1. Ag in 2 mbar H2
Sample mounted on a stainless steel holder using stainless steel clips
Sputter cleaned for 15 minutes using 3 kV Ar at a pressure of 1E-5 and 10 mA emission current
Ag foil measured in 2 mbar H2. Sample-to-nozzle distance was 0.8 mm. Nozzle diameter was 0.8 mm.
Ag
C
Ar
O
foil
Dataset Info

This will generate DOI for a single dataset
5
13-03-2020
Conditions
pressure
2
mbar
ambient composition
H2
none
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diammeter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
Ag MNN
2
Ag 3p
3
Ag 3d
4
Ag 4d
5
survey
Photon energy 1486.61eV
Spectrum type survey
Resolution 20
Dwell Time 0.4
Step size 0.5
Number of scans 1
Sample Info
1. Ag in vacuum
Sample mounted on a stainless steel holder using stainless steel clips
Sputter cleaned for 15 minutes using 3 kV Ar at a pressure of 1E-5 and 10 mA emission current
Ag foil measured in vacuum. Sample-to-nozzle distance was 0.8 mm. Nozzle diameter was 0.8 mm.
Ag
C
Ar
O
foil
Dataset Info

This will generate DOI for a single dataset
5
13-03-2020
Conditions
pressure
1E-8
mbar
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
survey
2
Au 4f
3
Au 4d
4
Au 4p
Photon energy 1486.61eV
Spectrum type Au 4p
Resolution 20
Dwell Time 0.1
Step size 0.1
Number of scans 1
Sample Info
2. Au in 2 mbar H2
Sample mounted on a stainless steel holder using stainless steel clips
Sputter cleaned for 15 minutes using 3 kV Ar at a pressure of 1E-5 and 10 mA emission current
Au foil measured in 2 mbar H2. Sample-to-nozzle distance was 0.8 mm. Nozzle diameter was 0.8 mm.
Au
C
Ar
foil
Dataset Info

This will generate DOI for a single dataset
4
12-03-2020
Conditions
pressure
2
mbar
ambient composition
H2
none
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
survey
2
Au 4f
3
Au 4d
4
Au 4p
Photon energy 1486.61eV
Spectrum type Au 4p
Resolution 20
Dwell Time 0.1
Step size 0.1
Number of scans 1
Sample Info
2. Au in vacuum
Sample mounted on a stainless steel holder using stainless steel clips
Sputter cleaned for 15 minutes using 3 kV Ar at a pressure of 1E-5 and 10 mA emission current
Au foil measured in vacuum. Sample-to-nozzle distance was 0.8 mm. Nozzle diameter was 0.8 mm.
Au
C
Ar
foil
Dataset Info

This will generate DOI for a single dataset
4
13-03-2020
Conditions
pressure
1E-8
mbar
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
survey
2
Cu 2p
3
Cu LMM
4
Cu 3s
5
Cu 2s
Photon energy 1486.61eV
Spectrum type Cu 2s
Resolution 20
Dwell Time 0.2
Step size 0.1
Number of scans 1
Sample Info
3. Cu in 2 mbar H2
Sample mounted on a stainless steel holder using stainless steel clips
Sputter cleaned for 15 minutes using 3 kV Ar at a pressure of 1E-5 and 10 mA emission current
Cu foil measured in 2 mbar H2. Sample-to-nozzle distance was 0.8 mm. Nozzle diameter was 0.8 mm.
Cu
C
Ar
O
foil
Dataset Info

This will generate DOI for a single dataset
5
12-03-2020
Conditions
pressure
2
mbar
ambient composition
H2
none
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
No
Element; Emission line;
1
survey
2
Cu 2p
3
Cu LMM
4
Cu 3s
5
Cu 2s
Photon energy 1486.61eV
Spectrum type Cu 2s
Resolution 20
Dwell Time 0.2
Step size 0.1
Number of scans 1
Sample Info
3. Cu in vacuum
Sample mounted on a stainless steel holder using stainless steel clips
Sputter cleaned for 15 minutes using 3 kV Ar at a pressure of 1E-5 and 10 mA emission current
Cu foil measured in vacuum. Sample-to-nozzle distance was 0.8 mm. Nozzle diameter was 0.8 mm.
Cu
C
Ar
O
foil
Dataset Info

This will generate DOI for a single dataset
5
12-03-2020
Conditions
pressure
1E-8
mbar
temperature
25
C
Spectrometer Settings
FAT
0.8 mm diameter
150 W, 15 kV
0.8 mm diameter
90 degrees
22 degrees
Calibration
ISO 15472:2010
Au 4f7/2
83.95
06-03-2020
Conductive
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