Ag0.98Pd0.02
Dataset Spectra
No
Element; Emission line;
Photon energy 485eV
Spectrum type Pd 3d
Resolution 8
Lens Mode ARM22
Dwell Time 0.1
Step size 0.05
Number of scans 10
Sample Metadata
Ag
Pd
foil
Name Ag0.98Pd0.02
Ex situ preparation Quantitative amounts of the Ag (slugs 3×3mm, 99.99%) and Pd (granules <7mm, 99.95%) purchased from EvoChem were melted in a light oven, with a four times re-melting process for homogenization. Afterwards the alloy was cold-rolled to a 1.6 mm thick foil and then annealed for 6h at 800°C to promote grain growth. The foil was cut into smaller pieces and mechanically polished step by step until a roughness 200 nm, by using an aluminium oxide polishing suspension as abrasive.
In situ preparation Ar+ sputter and annealing (in O2) cycles to clean the sample. The last step was Ar+ sputtering
Dataset Metadata
Measurement Date 05-06-2019
Measurement conditions
Condition Value Units
pressure 1E-8 mbar
Spectrometer Settings
Analyzer Mode FAT
Area
Strength
Source Beam Size
Take Off Angle 90
Analyzer Acceptance Angle
Contributor Info
Laboratory BelChem
Instrument Phoibos NAP-150
Contributors
Profile picture of Mark Greiner
Mark Greiner
Contributor
Profile picture of Caroline Hartwig
Caroline Hartwig
Owner
Calibration Info
Protocol ISO 15472:2010
Calibration date unknown
Calibration value
Emission line fermi
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Ag 00 0
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foil 00 0
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Pd 00 0
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Ag0.98Pd0.02 0
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